焦炭反应性现场试验工艺流程说明实物图片说明

注：本案例为现场实际应用案例，其中焦炭反应性测定装置型号为SYD-T222型，其中配套的反应器支架及反应管支架已升级为支架，带有不锈钢防护外套。
SYD-T222 基本配置：气电集成一体化控制仪，三相平衡供电；栏栅式硅碳棒（6组12棒）加热；自动升温恒温控制；自动气体切换控制；自动气体（CO2+N2）流量控制；
具体参数请参考本网站的产品展示。
本流程按GB/T4000-2008标准执行。
1、按GB/T4000-2008制取颗粒焦炭样
="zoom（this this.src）" alt=1.jpg src="http://www.sydch.com/bbs/attachments/month_1003/10030311243e7f16ab3d56e283.jpg" width=600 unselectable="true" y="345" x="567" file="attachments/month_1003/10030311243e7f16ab3d56e283.jpg" status="2" initialized="true" outfunc="null" w="600" h="338">

2、进烘箱烘干处理
="zoom（this this.src）" alt=2.jpg src="http://www.sydch.com/bbs/attachments/month_1003/1003031124a0281339077ea65e.jpg" width=600 unselectable="true" y="739" x="567" file="attachments/month_1003/1003031124a0281339077ea65e.jpg" status="2" initialized="true" outfunc="null" w="600" h="338">

3、烘干完成
="zoom（this this.src）" alt=3.jpg src="http://www.sydch.com/bbs/attachments/month_1003/10030311240e6f86a4d3ebced5.jpg" width=600 unselectable="true" y="1133" x="567" file="attachments/month_1003/10030311240e6f86a4d3ebced5.jpg" status="2" initialized="true" outfunc="null" w="600" h="338">

4、称量取200g
="zoom（this this.src）" alt=4.jpg src="http://www.sydch.com/bbs/attachments/month_1003/1003031124fea6ed393120ed0e.jpg" width=600 unselectable="true" y="1527" x="567" file="attachments/month_1003/1003031124fea6ed393120ed0e.jpg" status="2" initialized="true" outfunc="null" w="600" h="338">

5、反应器中分别装入高铝球、筛片
="zoom（this this.src）" alt=5.jpg src="http://www.sydch.com/bbs/attachments/month_1003/1003031124c896b985db8f7ef1.jpg" width=600 unselectable="true" y="1921" x="567" file="attachments/month_1003/1003031124c896b985db8f7ef1.jpg" status="2" initialized="true" outfunc="null" w="600" h="338">

6、再装入200g焦炭
="zoom（this this.src）" alt=6.jpg src="http://www.sydch.com/bbs/attachments/month_1003/1003031124e9945f0790a17490.jpg" width=600 unselectable="true" y="2315" x="567" file="attachments/month_1003/1003031124e9945f0790a17490.jpg" status="2" initialized="true" outfunc="null" w="600" h="338">

7、将装好试样的反应器置入反应炉中，并接好供气管路
="zoom（this this.src）" alt=7.jpg src="http://www.sydch.com/bbs/attachments/month_1003/100303112423b148b43d65fbab.jpg" width=600 unselectable="true" y="2709" x="567" file="attachments/month_1003/100303112423b148b43d65fbab.jpg" status="2" initialized="true" outfunc="null" w="600" h="338">

8、启动计算自动进入试验程序（SYD-T222）
="zoom（this this.src）" alt=8.jpg src="http://www.sydch.com/bbs/attachments/month_1003/100303112408eb2fce8308821a.jpg" width=600 unselectable="true" y="3103" x="567" file="attachments/month_1003/100303112408eb2fce8308821a.jpg" status="2" initialized="true" outfunc="null" w="600" h="338">

9、反应恒温停止并给出提示，提出反应器
="zoom（this this.src）" alt=9.jpg src="http://www.sydch.com/bbs/attachments/month_1003/100303112419f82eea0e0cc45a.jpg" width=600 unselectable="true" y="3497" x="567" file="attachments/month_1003/100303112419f82eea0e0cc45a.jpg" status="2" initialized="true" outfunc="null" w="600" h="338">

10、将反应器置于冷却架上自然冷却
="zoom（this this.src）" alt=10.jpg src="http://www.sydch.com/bbs/attachments/month_1003/100303112497899f87c3406e9d.jpg" width=600 unselectable="true" y="3891" x="567" file="attachments/month_1003/100303112497899f87c3406e9d.jpg" status="2" initialized="true" outfunc="null" w="600" h="338">

11、温度降至100度以下后，自动给出提示，此时打开反应器
="zoom（this this.src）" alt=11.jpg src="http://www.sydch.com/bbs/attachments/month_1003/1003031124f0919e425539e3f3.jpg" width=600 unselectable="true" y="4285" x="567" file="attachments/month_1003/1003031124f0919e425539e3f3.jpg" status="2" initialized="true" outfunc="null" w="600" h="338">

12、倒出反应器中的混合物，分离焦炭、高铝球、筛片
="zoom（this this.src）" alt=12.jpg src="http://www.sydch.com/bbs/attachments/month_1003/10030311243b7e632d6ad2c74a.jpg" width=600 unselectable="true" y="4679" x="567" file="attachments/month_1003/10030311243b7e632d6ad2c74a.jpg" status="2" initialized="true" outfunc="null" w="600" h="338">

13、称量反应后的剩余残留
="zoom（this this.src）" alt=13.jpg src="http://www.sydch.com/bbs/attachments/month_1003/10030311243e2fd7fde4398f8c.jpg" width=600 unselectable="true" y="5073" x="567" file="attachments/month_1003/10030311243e2fd7fde4398f8c.jpg" status="2" initialized="true" outfunc="null" w="600" h="338">

14、入I型转鼓进行强度试验，然后筛分后得到称量数值填入计算机，将自动给出终试验报告，结束试验！
="zoom（this this.src）" alt=14.jpg src="http://www.sydch.com/bbs/attachments/month_1003/1003031124fd203a7fc3cf4dbf.jpg" width=600 unselectable="true" y="5467" x="567" file="attachments/month_1003/1003031124fd203a7fc3cf4dbf.jpg" status="2" initialized="true" outfunc="null" w="600" h="375">